Optical and Structural Properties of Nanopowders of Lead Compounds Obtained by the Electrochemical Method


  • B.D. Nechyporuk Rivne State Humanitarian University
  • O.F. Kolomys V.E. Lashkaryov Institute of Semiconductor Physics, Nat. Acad. of Sci. of Ukraine
  • B.P. Rudyk National University of Water Management and Nature Resources
  • V.V. Strelchuk V.E. Lashkaryov Institute of Semiconductor Physics, Nat. Acad. of Sci. of Ukraine
  • M.V. Moroz National University of Water Management and Nature Resources
  • V.O. Myslinchyk Rivne State Humanitarian University
  • B.A. Tataryn Lesya Ukrainka Volyn National University




α- and β-lead oxides, lead carbonate, XRD structural studies, nanoparticle size, Debye–Scherrer formula, Raman scattering, photoluminescence


The influence of the temperature and electrolyte composition on the synthesis of nanopowders of lead compounds using the electrochemical method has been studied. X-ray diffraction (XRD) studies were carried out, and their results are used to determine the composition of obtained specimens and the size of nanocrystallites in them (using the Debye–Scherrer formula). The possibility of the formation of lead oxides and lead carbonate, when electrochemically synthesizing nanoparticles is discussed. It is shown that a mixture of lead oxide and lead carbonate nanocrystals is obtained irrespective of the electrolyte temperature. The results of XRD structural studies are compared with the results of Raman studies of the same specimens. The photoluminescence bands of synthesized compounds are analyzed.


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How to Cite

Nechyporuk, B., Kolomys, O., Rudyk, B., Strelchuk, V., Moroz, M., Myslinchyk, V., & Tataryn, B. (2024). Optical and Structural Properties of Nanopowders of Lead Compounds Obtained by the Electrochemical Method. Ukrainian Journal of Physics, 69(5), 349. https://doi.org/10.15407/ujpe69.5.349



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